This practice-oriented textbook teaches how to use magnetic resonance spectroscopy - one of the most powerful analytical methods available showing how to utilize the huge variety of NMR experiments available today in addition to the standard experiments. The book is intended as a practical guide for students and laboratory personnel. Therefore, the emphasis is on practical rather than on theoretical aspects, which are treated only to the extent necessary to understand the experiments and to interpret the results.

The book has been significantly revised and expanded for the 2nd edition, and now includes the nuclei 1 H/ 2 H, 13 C, 31 P, 17 O, 15 N, 19 F, 29 Si, 77 Se, 113 Cd, 117 Sn/ 119 Sn, 195 Pt, 207 Pb and a new chapter on solid state NMR. An expanded set of 50 graded problems in the problems section supports understanding of how problems in structure elucidation are solved by using NMR offers invaluable help for students, practitioners and laboratory personnel alike.

The practical guide to today's NMR experiments aims at teaching how to use the huge variety of NMR experiments available today The emphasis is on practical rather than on theoretical aspects Now includes the nuclei 1H/2H, 13C, 31P, 17O, 15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb and a new chapter on solid state NMR The collection of 50 problems of different complexity is an invaluable help for students, practitioners and laboratory personnel Includes supplementary material: sn.pub/extras

Autorentext

Introduction Part I - NMR Experiments 1. 1D Experiments 2. 2D Experiments 3. Quadrupolar Nucleus Experiments 4. HPLC-NMR Coupling Appendix: Reference List Part II - Worked Example and Problems Introduction Worked Example Problems Index

Inhalt
NMR Experiments.- 1D Experiments.- 2D Experiments.- Quadrupolar Nucleus Experiments.- HPLC-NMR Coupling.- Other Spin-1/2 Nuclei.- Solid State NMR.- Worked Example and Problems.- Section 1.- Worked Example.- Problems.- Section 2.