This practice-oriented textbook teaches how to use magnetic resonance spectroscopy - one of the most powerful analytical methods available - showing how to utilize the huge variety of NMR experiments available today in addition to the standard experiments. The book is intended as a practical guide for students and laboratory personnel. Therefore, the emphasis is on practical rather than on theoretical aspects, which are treated only to the extent necessary to understand the experiments and to interpret the results.

The book has been significantly revised and expanded for the 2nd edition, and now includes the nuclei 1H/2H, 13C, 31P, 17O, 15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb and a new chapter on solid state NMR. An expanded set of 50 graded problems in the problems section supports understanding of how problems in structure elucidation are solved by using NMR offers invaluable help for students, practitioners and laboratory personnel alike.

Autorentext

Introduction

Part I - NMR Experiments

1. 1D Experiments

2. 2D Experiments

3. Quadrupolar Nucleus Experiments

4. HPLC-NMR Coupling

Appendix: Reference List

Part II - Worked Example and Problems

Introduction

Worked Example

Problems

Index

Klappentext

This practice-oriented textbook shows how to utilize the huge variety of NMR experiments available today in addition to standard experiments. Intended as a practical guide for students and laboratory personnel, it treats theoretical aspects only to the extent necessary to understand the experiments and to interpret the results.

The book is significantly revised and expanded for the 2nd edition, and now includes the nuclei 1H/2H, 13C, 31P, 17O, 15N, 19F, 29Si, 77Se, 113Cd, 117Sn/119Sn, 195Pt, 207Pb and a new chapter on solid state NMR. An expanded set of 50 graded problems offers invaluable help for students, practitioners and laboratory personnel alike.

Inhalt

Introduction.- Part I - NMR Experiments.- 1D Experiments.- 2D Experiments.- Quadrupolar Nucleus.- Experiments.- HPLC-NMR Coupling.- Appendix: Reference List.- Part II - Worked Example and Problems.- Introduction.- Worked Example.- Problems.