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Methods for Structure Elucidation by High-Resolution NMR: Applications to Organic Molecules of Moderate Molecular Weight

  • Livre Relié
  • 356 Nombre de pages
Nuclear Magnetic Resonance Spectroscopy (NMR) is widely regarded as having evolved into a subscience. This book focuses on the dev... Lire la suite
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Description

Nuclear Magnetic Resonance Spectroscopy (NMR) is widely regarded as having evolved into a subscience. This book focuses on the developments in the field of high resolution NMR, with a view to applications on the structure elucidation of organic molecules of moderate molecular weight. It is suitable for chemists and application NMR scientists.

Texte du rabat

Each chapter is a unique synthesis of the authors' previous research results in the given field, and thus projects special insights. Much emphasis has been given to the latest developments in NMR, in particular to selective pulses and pulsed field gradients. As a part of the series "Analytical Spectroscopy Library", with subsequent editions coming along this book should provide a platform for future research accounts of similar flavor. The material is presented in a mostly non-mathematical fashion, and is intended mainly for chemists, application NMR scientists and students with already some background in NMR. Some of the chapters slightly overlap in the discussed topics, which is particularly exciting in terms of gaining insight into the same area from different angles.

Contenu

Preface. Contents. List of contributors. Selective pulses in NMR (S.J.F. Vincent, C. Zwahlen). Multiple selective excitation: a method to improve the efficiency of selective 1D and 2D experiments (P. Bigler). Concatenation of polarization transfer steps in 1D homonuclear chemical shift correlated experiments. Application to oligo- and polysaccharides (D. Uhrin). The selective reverse INEPT experiment (G.A. Morris, I.C. Clements). GROESY, gradient-enhanced selective 1D ROE measurements (P. Adell et al.). The DANTE-Z experiment (D. Canet, C. Roumestand). One-dimensional TOCSY and related 1D techniques (T.C. Wong). Use of high-power spin-lock purge pulses in high-resolution NMR spectroscopy (G. Otting). Decoupled HMBC (D-HMBC), an improved version of HMBC (H. Seto, K. Furihata). Optimal acquisition and presentation of HoMQC spectra (I. Pelczer, K.D. Bishop). High resolution diffusion ordered spectroscopy (G.A. Morris, H. Barjat). Chemical exchange measurements in NMR (A.D. Bain). Homonuclear two-dimensional cross-relaxation spectroscopy (N. Juranic et al.). Reference deconvolution (G.A. Morris, H. Barjat). The super fast inversion recovery (SUFIR) experiment (D. Canet et al.). Measurements of relaxation rates for low natural abundance I=1/2 nuclei (J. Kowalewski, L. Maler).

Détails sur le produit

Titre: Methods for Structure Elucidation by High-Resolution NMR: Applications to Organic Molecules of Moderate Molecular Weight
Sous-titre: Applications to Organic Molecules of Moderate Molecular Weight
Éditeur:
Code EAN: 9780444821577
ISBN: 978-0-444-82157-7
Format: Livre Relié
Editeur: Elsevier New York
Genre: Chimie
nombre de pages: 356
Poids: 689g
Taille: H234mm x B156mm x T21mm
Année: 1997