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Modified Graphene Oxide and its Uses as Electrochemical Sensor

  • Kartonierter Einband
  • 208 Seiten
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This study involved preparation of graphene oxide (GO) and reduced graphene oxide (RGO) using Hummer method and chemical method re... Weiterlesen
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Beschreibung

This study involved preparation of graphene oxide (GO) and reduced graphene oxide (RGO) using Hummer method and chemical method respectively. These carbon nanomaterials were used as starting material to make novel functionalize with thiocarbohydrazide (TCH) which was prepared by reacting CS2 with hydrazine to form GO or RGO- 4-amino,5-substituted 1H,1,2,4 triazole 5(4H) thion (ASTT) , (GOT) and( RGOT) respectively via cyclocondensation reaction. Also MnO2 nanorod was prepared to form hybridized with GOT and RGOT. A commercial multiwall carbon nanotube (MWCNT) and functionalization with carboxylic groups' (f-MWCNT) and its nanocomposite with GOT were also prepared. All carbon nanomaterials were characterized with different techniques such as Fourier transform infrared (FT-IR), X-ray diffraction (XRD), atomic force microscope (AFM) scanning electron microscope (SEM) and elemental analysis. XRD showed presence diffraction peak at 11.95 for GO and this diffraction disappeared for RGO. Diffraction peak of crystal planes for MnO2 matched well with standard data. The diameter of MnO2 nanotubes was determined using Debye Scherer equation and found to be 11.6 nm.

Autorentext
Abdalkreem, Issam A. Issam Abdalkreem, Ph.D. and M.Sc. of Physical Chemistry from Martin-Luther University Halle-Wittenberg, Germany. B.Sc. of Chemistry from University of Sulaimani, Iraq. He is currently Assistant Professor of Physical Chemistry at Baghdad University, Baghdad, Iraq.

Produktinformationen

Titel: Modified Graphene Oxide and its Uses as Electrochemical Sensor
Untertitel: Synthesis of Modified Graphene Oxide and its Application as Electrochemical Sensor
Autor:
EAN: 9786139938308
ISBN: 978-613-9-93830-8
Format: Kartonierter Einband
Genre: Chemie
Anzahl Seiten: 208
Gewicht: g
Größe: H220mm x B220mm x T150mm
Veröffentlichung: 27.12.2018
Jahr: 2018